①应适当调整冰乙酸加入量,使A测定处于0.1-0.8之间可提高结果准确性,计算时相应修改;
②试剂一和冰乙酸具有刺激性和挥发性,高氯酸具有强腐蚀性,操作时请做好防护措施;
③加热过程需严格密封,以防气体溢出,加热过程伴随有剧烈反应,混匀时应缓慢轻摇,以免压力过大喷出造成伤害;
④若玻璃试管操作不方便,可使用带盖密封性较好的离心管作为反应容器,请确保无橡胶等易腐蚀材质,以免造成泄漏;
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